Temperature Resistance Properties of Unidirectional Laminated C f/SiC-Al Prepared by PIP and Vacuum Pressure Infiltration

Materials (Basel). 2023 Aug 3;16(15):5445. doi: 10.3390/ma16155445.

Abstract

Material used for aero-engine fan blade requires excellent mechanical properties at high temperature (300 °C). Continuous carbon-fiber-reinforced silicon carbide ceramic matrix composites (Cf/SiC) are necessary candidates in this field, possessing low density, high strength, high modulus, and excellent high-temperature resistance. However, during the preparation process of Cf/SiC, there were inevitably residual pores and defects inside, resulting in insufficient compressive strength and reliability. The vacuum pressure melting infiltration process was used to infiltrate low melting point and high wettability aluminum alloys into the porous Cf/SiC composite material prepared by the precursor impregnation cracking process, repairing the residual pore defects inside the body. The porosity of porous Cf/SiC decreased from 49.65% to 5.1% after aluminum alloy repair and strengthening. The mechanical properties of Cf/SiC-Al composite materials strengthened by aluminum alloy repair after heat treatment were studied. The tensile strength of the as-prepared Cf/SiC-Al was 166 ± 10 MPa, which were degraded by 13~22% after heat treatment. The nonlinear sections of stress-displacement curve of as-treated samples were shorter than that of as-prepared sample. The hardness of aluminum alloy matrix after 300 °C 1 h heat treatment was 58 Hv, which was not obviously reduced compared with the sample without heat treatment. The vacuum infiltration of aluminum alloy is expected to have guiding significance for repairing and strengthening internal defects in ceramic matrix composites.

Keywords: Cf/SiC-Al; heat treatment; mechanical properties; microstructure.