An Experimental Study on the Healing Performance of Complex Capsules Using Multiphase Inorganic Materials for Crack Self-Healing of Cement Mortars

Materials (Basel). 2022 Dec 9;15(24):8819. doi: 10.3390/ma15248819.

Abstract

Recently, a self-healing technique capable of repairing cracks in structures has emerged. Among various self-healing technologies, self-healing capsules can be largely classified into two types, depending on the phase of the core material: solid capsules, in which the core material is a powder; and microcapsules, in which the core material is a liquid. Solid capsules and microcapsules have different mechanisms, and their capsule sizes are also distinctly different. This suggests that each has advantages and disadvantages. Most of the studies known to date have utilized single capsules. However, if one uses a mixture of the two types of capsules, it is possible to highlight the strengths of each capsule and compensate for the weaknesses. Therefore, in this study, the first research on complex capsules that mixed solid capsules and microcapsules was attempted. As a result of the experiment, the complex capsule slightly reduced the fluidity of the mortar, but the effect was not significant. Moreover, the complex capsule tended to reduce the compressive strength of the mortar. In particular, it was found that the effect of solid capsules on the reduction in compressive strength among complex capsules was greater than that of microcapsules. Conversely, the healing performance increased when the ratio of solid capsules in the complex capsules was large.

Keywords: cement mortar; complex capsules; crack; healing performance; inorganic materials; multiphase; self-healing.