Extraction of phase information approximating the demagnetization field within a thin-foiled magnet using electron holography observation

Microscopy (Oxf). 2023 Aug 4;72(4):343-352. doi: 10.1093/jmicro/dfac066.

Abstract

This paper proposes a method that provides a phase image related to the demagnetization field (Hd) within a thin-foil permanent magnet using electron holography. The observation of Hd remains a significant challenge because electron holography in principle allows only imaging of the magnetic flux density (B), which is a mixture of the contributions from magnetization (M), stray magnetic field (Hs) outside of the specimen and Hd inside of the specimen. The phase map approximating Hd, which was determined by processing of the electron holography observation from a Nd2Fe14B single-crystalline specimen, showed a good agreement with the prediction by micromagnetic theory. With respect to permanent magnets, this method can be applied to examinations about the coercivity mechanism, which is sensitive to the demagnetization field. Graphical Abstract.

Keywords: coercivity; demagnetization; electron holography; electron microscopy; nucleation of reverse magnetic domains; permanent magnet.