Ultrasound characterization of the viscoelastic properties of additively manufactured photopolymer materials

J Acoust Soc Am. 2022 Sep;152(3):1901. doi: 10.1121/10.0014180.

Abstract

Photopolymer-based additive manufacturing has received increasing attention in the field of acoustics over the past decade, specifically towards the design of tissue-mimicking phantoms and passive components for ultrasound imaging and therapy. While these applications rely on an accurate characterization of the longitudinal bulk properties of the materials, emerging applications involving periodic micro-architectured media also require the knowledge of the transverse bulk properties to achieve the desired acoustic behavior. However, a robust knowledge of these properties is still lacking for such attenuating materials. Here, we report on the longitudinal and transverse bulk properties, i.e., frequency-dependent phase velocities and attenuations, of photopolymer materials, which were characterized in the MHz regime using a double through-transmission method in oblique incidence. Samples were fabricated using two different printing technologies (stereolithography and polyjet) to assess the impact of two important factors of the manufacturing process: curing and material mixing. Overall, the experimentally observed dispersion and attenuation could be satisfactorily modeled using a power law attenuation to identify a reduced number of intrinsic ultrasound parameters. As a result, these parameters, and especially those reflecting transverse bulk properties, were shown to be very sensitive to slight variations of the manufacturing process.