Studying the Effect of Cold Rolling and Heat Treatment on the Microstructure and Mechanical Properties of the Fe36Mn20Ni20Cr16Al5Si3 High Entropy Alloy

Essam R I Mahmoud; Awaludin Shaharoun; Mohamed A Gepreel; Saad Ebied

doi:10.3390/e24081040

Studying the Effect of Cold Rolling and Heat Treatment on the Microstructure and Mechanical Properties of the Fe₃₆Mn₂₀Ni₂₀Cr₁₆Al₅Si₃ High Entropy Alloy

Entropy (Basel). 2022 Jul 28;24(8):1040. doi: 10.3390/e24081040.

Authors

Essam R I Mahmoud¹, Awaludin Shaharoun¹, Mohamed A Gepreel², Saad Ebied³

Affiliations

¹ Department of Mechanical Engineering, Islamic University of Madinah, Madinah 42351, Saudi Arabia.
² Materials Science and Engineering Department, Egypt-Japan University of Science and Technology, Alexandria 21934, Egypt.
³ Department of Production Engineering and Mechanical Design, Faculty of Engineering, Tanta University, Tanta 31527, Egypt.

Abstract

In this study, a multi-component FeMnNiCrAlSi high-entropy alloy, chosen through Thermo-Calc^® software (2021a, Stockholm, Sweden) calculation and produced by electric arc melting, was studied for phase continents and mechanical properties. The results elucidated that the cold rolled condition (area reduction ratio about 86%) was in the form of elongated grains with a dendritic structure. Also, small amounts of the BCC phase were precipitated at the grain boundaries. The annealed sample shows features of BCC phase and different sizes of intermetallics. These results coincided with the predictions of Thermo-Calc^® software calculations. A cold rolled sample showed high compressive yield strength of about 950 MPa, and the annealed sample had only half the strength of the cold rolled condition. The cold rolled sample shows the highest micro-hardness. The wear resistance of the annealed condition was significantly improved at room temperature and at 200 °C. The brittle phases in the annealed condition have a positive impact on the wear resistance.

Keywords: casting; high entropy alloys; microstructure; thermomechanical processing; wear resistance.

Grants and funding

This research received no external funding.