Crack-Resistant Cements under Drying: Results from Ring Shrinkage Tests and Multi-Physical Modeling

Materials (Basel). 2022 Jun 7;15(12):4040. doi: 10.3390/ma15124040.

Abstract

Cementitious materials exhibit shrinkage strain on drying, leading easily to crack formation when internally or externally restrained. It is known that cements with a slow strength gain show higher crack resistance under external drying. The ring shrinkage test can be considered an accelerated method for cracking tendency due to existing historical correlations between ring cracking time and long-term surface concrete cracking. The experimental campaign used ring shrinkage tests on 25 mortars, covering 10 commercial cements and 15 cements produced on demand, covering Portland cements and blended cements up to a 30% slag substitution. The results show that the restrained ring cracking time generally increases with lower Blaine fineness and higher slag substitution in 6 to over 207 days' span. Upper limits for crack-resistant cements were proposed for 2-day compressive strength and Blaine fineness, in the case of Portland cements: 27.7 MPa and 290 m2/kg, respectively. A hygro-mechanical model successfully replicated strain evolution with crack formation and brittle failure. Only two out of ten commercial cements were classified as crack-resistant, while the ratio increased to 10 out of 15 cements which were produced on demand.

Keywords: chemical shrinkage; crack-resistant cements; cracking; creep; drying shrinkage; hygro-mechanical simulation; ring shrinkage test; strength gain.