Effect of Intercritical Annealing Time on Microstructure Evolution and Mechanical Properties of Low Carbon Medium Manganese Steel Subjected to Multi-Step Heat Treatment Process

Materials (Basel). 2022 Mar 25;15(7):2425. doi: 10.3390/ma15072425.

Abstract

A novel multi-step heat treatment process was performed for 0.2C-5Mn steel, and the effect of intercritical annealing (IA) durations on the microstructure evolution and mechanical properties was studied. The results showed that the content of primary reversed austenite (PRA) hardly changed as the IA time increased from 6 h to 50 h, but only less than 10% of PRA remained after being tempered at 200 °C due to the appearance of secondary martensite (SM). The final microstructure contained SM, the primary martensite (PM), and RA, which was protected by the SM so that the transformation-induced plasticity (TRIP) effect was unlikely to occur. Meanwhile, the (Ti, V, Mo)C particle sizes were 14.27, 14.68 and 15.65 nm for the intermediate processes of IA-6 h, IA-12 h, and IA-50 h, respectively. As the IA time increased from 6 h to 50 h, both the dislocation and precipitation strengthening increment decreased. As a result, the best mechanical properties were obtained from the intermediate process of IA-12 h, with a yield strength of 1115.5 MPa, tensile strength of 1573.5 MPa, and -20 °C impact energy of 30.4 J.

Keywords: intercritical annealing time; mechanical properties; medium manganese steel; microstructure; multi-step heat treatment process; reversed austenite.