Polymer Microtip on a Multimode Optical Fiber as a Threshold Volatile Organic Compounds Sensor

Sensors (Basel). 2022 Feb 7;22(3):1246. doi: 10.3390/s22031246.

Abstract

Polymer microtips are 3D microstructures manufactured on the end face of an optical fiber by using the photopolymerization process. Such micro-optic elements made on a multi-mode optical fiber were previously tested as a transducer of refractive index sensor. These studies were an inspiration to investigate the possibility of using this type of transducer to measure the presence of volatile organic compounds in the air. The experimental results of microtips polymerized with UV and VIS were reported. It was possible to detect the presence of five different volatile compounds in the air due to the sensitivity of the transducer to the refractive indices changes. These changes were induced by the vapors condensed on the microtip surface. The measured time responses have shown that the return loss decreases rapidly as the microtip is inserted inside a glass vial filled with the tested compound. Moreover, correlations between calculated dynamic ranges and refractive indices and volumes of the volatile compounds inside the vials were negligible. Therefore, this type of sensor can be categorized as a condensed material threshold sensor. This sensor can be used in warning systems for monitoring leakages of pipelines carrying volatile chemicals.

Keywords: optical fiber refractive index sensors; photopolymerization; vapor detection.