Preparation and characterization of non-crystalline granular starch with low processing viscosity

Int J Biol Macromol. 2022 Jan 15:195:483-491. doi: 10.1016/j.ijbiomac.2021.12.053. Epub 2021 Dec 14.

Abstract

Non-crystalline granular starch (NCGS) has advantages in the deep processing of starch owing to its unique structure and function. In this study, NCGS was successfully prepared at a baking temperature of 210 °C, and the morphology, structure, pasting properties, and rheological properties of the NCGS were systematically studied. Compared with native starch, NCGS showed a lower processing viscosity and rapid reduction in the peak viscosity from 3795 to 147 cP. Furthermore, NCGS exhibited impaired short- and long-range ordered structures, as indicated by the lower ratio of absorbance at 1047/1015 cm-1 and decreased crystallinity compared to native starch. Additionally, amylose and amylopectin with long and medium chains in NCGS were degraded into short chains, resulting in an increase in amylose content and branch density. The analysis of the physicochemical properties of NCGS, especially the low processing viscosity, is of great importance for the industrial application of starch, particularly in terms of improving the yield, saving energy, and reducing environmental pollution.

Keywords: High-temperature treatment; Low processing viscosity; Non-crystalline granular starch; Structure.

MeSH terms

  • Chemical Phenomena*
  • Rheology
  • Spectrum Analysis
  • Starch / chemistry*
  • Starch / isolation & purification*
  • Starch / ultrastructure
  • Temperature
  • Viscosity*

Substances

  • Starch