Evaluation of Microshear Bond Strength of Four Different CAD-CAM Polymer-Infiltrated Ceramic Materials after Thermocycling

J Prosthodont. 2022 Aug;31(7):623-628. doi: 10.1111/jopr.13469. Epub 2022 Jan 6.

Abstract

Purpose: To evaluate the bond strength of three monolithic hybrid ceramics/resin nanoceramics and a zirconia-reinforced lithium silicate to resin cement after thermocycling.

Materials and methods: Using four materials, including Vita Enamic (VITA Zahnfabrik), Lava Ultimate (3M ESPE), Crystal Ultra (Digital Dental), and Vita Suprinity (VITA Zahnfabrik), 64 specimens were prepared with dimensions of 4 mm × 3 mm × 1.5 mm. Vita Suprinity samples were sintered at 840°C for 8 min. After polishing and cleaning all the samples in each group (n = 16), they were subjected to their recommended surface treatment: 10% hydrofluoric acid for Vita Enamic (60s) and Vita Suprinity (20s); air abrasion of Lava Ultimate and Crystal Ultra with 50 u Al2 O3 particles. Then, tygon tubes were filled with dual cure resin cement (Panavia F2.0), cured and then subjected to thermal cycling (2000 cycles; 5-55°C). The microshear bond strength was measured using microtensile testing machine. The data were analyzed using Welch and Games-Howell tests (α = 0.05). The mode of failure was also evaluated using a stereomicroscope.

Results: The highest and the lowest mean microshear bond strength belonged to the Crystal Ultra (7.71 ± 1.54 MPa) and Vita Suprinity (4.73 ± 1.87 MPa) groups, respectively. The differences between groups were significant and Crystal Ultra had higher bond strength in comparison to all three materials (p < 0.05).

Conclusion: Hybrid ceramics showed higher bond strength to resin cements in comparison to resin nanoceramics and zirconia-reinforced lithium silicate materials.

Keywords: Hybrid ceramic; microshear bond strength; polymer-infiltrated ceramic network; resin cement; resin nanoceramic; zirconia-reinforced lithium silicate.

MeSH terms

  • Air Abrasion, Dental
  • Ceramics / chemistry
  • Computer-Aided Design
  • Dental Bonding*
  • Dental Porcelain* / chemistry
  • Dental Stress Analysis
  • Lithium
  • Materials Testing
  • Polymers
  • Resin Cements / chemistry
  • Silicates
  • Surface Properties

Substances

  • Polymers
  • Resin Cements
  • Silicates
  • Dental Porcelain
  • Lithium