Recent Materials Developed for Dispersive Solid Phase Extraction

Molecules. 2020 Oct 22;25(21):4869. doi: 10.3390/molecules25214869.

Abstract

Solid phase extraction (SPE) is an analytical procedure developed with the purpose of separating a target analyte from a complex sample matrix prior to quantitative or qualitative determination. The purpose of such treatment is twofold: elimination of matrix constituents that could interfere with the detection process or even damage analytical equipment as well as enriching the analyte in the sample so that it is readily available for detection. Dispersive solid phase extraction (dSPE) is a recent development of the standard SPE technique that is attracting growing attention due to its remarkable simplicity, short extraction time and low requirement for solvent expenditure, accompanied by high effectiveness and wide applicability. This review aims to thoroughly survey recently conducted analytical studies focusing on methods utilizing novel, interesting nanomaterials as dSPE sorbents, as well as known materials that have been only recently successfully applied in dSPE techniques, and evaluate their performance and suitability based on comparison with previously reported analytical procedures.

Keywords: dispersive solid phase extraction; environmental samples; food samples; nanomaterials; novel sorbents.

Publication types

  • Review

MeSH terms

  • Adsorption
  • Biological Products / isolation & purification
  • Carbon / chemistry*
  • Chromatography, High Pressure Liquid
  • Environmental Pollutants / isolation & purification
  • Food Analysis / methods
  • Hydroxides / chemistry
  • Metal-Organic Frameworks / chemistry*
  • Metals, Rare Earth / isolation & purification
  • Molecularly Imprinted Polymers / chemistry*
  • Nanostructures / chemistry*
  • Phosphoproteins / isolation & purification
  • Porosity
  • Silicon Dioxide / chemistry*
  • Solid Phase Extraction / methods*
  • Solvents / chemistry

Substances

  • Biological Products
  • Environmental Pollutants
  • Hydroxides
  • Metal-Organic Frameworks
  • Metals, Rare Earth
  • Molecularly Imprinted Polymers
  • Phosphoproteins
  • Solvents
  • Carbon
  • Silicon Dioxide