Purpose: The purpose of this study was to study the influence of high-pressure (HP) polymerization on the mechanical properties of denture base PMMA resins compared with conventional thermopolymerization and PMMA discs for digital dentures.
Materials and methods: Three groups of blocks were prepared: Probase Hot (Ivoclar Vivadent, Lichtenstein) conventionally heat polymerized at 100°C, Probase Hot heat polymerized at 100°C under HP (200 MPa) and Ivobase CAD (Ivoclar Vivadent, Lichtenstein). Samples for mechanical/physical (n = 30) and samples for viscoelastic (n = 10) characterizations were cut from the blocks. Flexural strength (σf ), elastic modulus (Ef ), hardness, density (ρ), flexural deformation at maximal flexural stress, flexural load energy (Ur ) and viscoelastic properties (E', E'', Tanδ, Tg ) were analyzed using one-way ANOVA (α = 0.05), Scheffé multiple means comparisons (α = 0.05) and Weibull statistics (for σf ). SEM images of the fractured surfaces were obtained.
Results: Ef , E', E'' and density of HP polymerized Probase hot were significantly higher than conventional heat polymerized Probase Hot, whereas Tg was significantly lower and σf , Tanδ, hardness, flexural deformation at maximal flexural stress, Ur were not significantly different. The highest values for σf , flexural deformation at maximal flexural stress, Ur and Weibull modulus were obtained with Ivobase CAD.
Conclusion: HP polymerization does not significantly increase the mechanical properties of denture base resins.
Keywords: PMMA denture base; Prosthetic dentistry/prosthodontics; high pressure polymerization; materials science(s); mechanical properties; viscoelastic properties.
© 2020 by the American College of Prosthodontists.