Sliding electrical contact exists in various electrical equipment. However, its performance is significantly affected by the sliding condition such as the load, electricity, and the surface state of friction pairs. In this study, a novel instrument is designed and constructed for high-frequency microforce electrical sliding friction testing. The new instrument provides a unique experimental platform that enables high-frequency reciprocating friction and microforce loading, and it has an innovative data collection system that includes a cantilever beam structure to measure the microforce. In this instrument, parameters (positive force, friction, displacement, and voltage of frictional pair) are obtained and monitored in real time. The steel sheet and nickel-plated steel wire were used as materials to conduct an experiment, and the steel sheet morphology after the experiment was observed using a light microscope. Results show that the voltage and positive load significantly influence the friction coefficient and friction wear, which is crucial in understanding friction and wear behaviors.