Dynamic nanoindentation testing: is there an influence on a material's hardness?

Mater Res Lett. 2017 Nov 3;5(7):486-493. doi: 10.1080/21663831.2017.1331384. eCollection 2017 Nov.

Abstract

Modern nanoindentation devices are capable of dynamic experimentations, which allow us to exploit instrumented hardness tests extensively. Beside the assets of recording mechanical properties continuously over displacement, there are ongoing debates whether the superimposed force alters the material's hardness. We will show for a broad range of materials that significant hardness differences are noted between dynamic and static tests, even for large displacements. Those mainly result from a changing indentation strain-rate during the hold segment at peak load. This fact must be implicitly considered in studies using static indentation tests to guarantee comparability of obtained nanoindentation hardness values and derived quantities.

Keywords: Nanoindentation; dynamic indentation testing; mechanical properties; strain-rate sensitivity.

Grants and funding

Funding by the Austrian Federal Government (837900), in particular from the Bundesministerium für Verkehr, Innovation und Technologie and the Bundesministerium für Wirtschaft, Familie und Jugend, represented by Österreichische Forschungsförderungsgesellschaft mbH and the Styrian and Tyrolean Provincial Government, represented by Steirische Wirtschaftsförderungsgesellschaft mbH and Standortagentur Tirol, within the framework of the COMET Funding Programme (MPPE, A7.19) is appreciated. Furthermore, parts of this work were also funded by the Austrian Science Fund (FWF) via the project P25325-N20.