SUT-NANOTEC-SLRI beamline for X-ray absorption spectroscopy

J Synchrotron Radiat. 2017 May 1;24(Pt 3):707-716. doi: 10.1107/S1600577517004830. Epub 2017 Apr 4.

Abstract

The SUT-NANOTEC-SLRI beamline was constructed in 2012 as the flagship of the SUT-NANOTEC-SLRI Joint Research Facility for Synchrotron Utilization, co-established by Suranaree University of Technology (SUT), National Nanotechnology Center (NANOTEC) and Synchrotron Light Research Institute (SLRI). It is an intermediate-energy X-ray absorption spectroscopy (XAS) beamline at SLRI. The beamline delivers an unfocused monochromatic X-ray beam of tunable photon energy (1.25-10 keV). The maximum normal incident beam size is 13 mm (width) × 1 mm (height) with a photon flux of 3 × 108 to 2 × 1010 photons s-1 (100 mA)-1 varying across photon energies. Details of the beamline and XAS instrumentation are described. To demonstrate the beamline performance, K-edge XANES spectra of MgO, Al2O3, S8, FeS, FeSO4, Cu, Cu2O and CuO, and EXAFS spectra of Cu and CuO are presented.

Keywords: Al K-edge XANES; Cu K-edge XANES; Mg K-edge XANES; S K-edge XANES; X-ray absorption spectroscopy; XAS beamline; intermediate-energy X-ray beamline.

Publication types

  • Research Support, U.S. Gov't, Non-P.H.S.
  • Research Support, Non-U.S. Gov't