High-temperature MAS-NMR at high spinning speeds

Holger Kirchhain; Julian Holzinger; Adrian Mainka; Andreas Spörhase; Sabarinathan Venkatachalam; Achim Wixforth; Leo van Wüllen

doi:10.1016/j.ssnmr.2016.06.003

High-temperature MAS-NMR at high spinning speeds

Solid State Nucl Magn Reson. 2016 Sep:78:37-39. doi: 10.1016/j.ssnmr.2016.06.003. Epub 2016 Jun 27.

Authors

Holger Kirchhain¹, Julian Holzinger¹, Adrian Mainka¹, Andreas Spörhase¹, Sabarinathan Venkatachalam¹, Achim Wixforth¹, Leo van Wüllen¹

Affiliation

¹ University of Augsburg, Institute of Physics, Universitätsstr. 1, 86159 Augsburg, Germany.

PMID: 27423513
DOI: 10.1016/j.ssnmr.2016.06.003

Abstract

A low cost version to enable high temperature MAS NMR experiments at temperatures of up to 700°C and spinning speeds of up to 10kHz is presented. The method relies on inductive heating using a metal coated rotor insert. The metal coating is accomplished via a two step process involving physical vapor deposition and galvanization.

Publication types

Letter
Research Support, Non-U.S. Gov't