Finding the Needle in the Haystack: Characterization of Trace Crystallinity in a Commercial Formulation of Paclitaxel Protein-Bound Particles by Raman Spectroscopy Enabled by Second Harmonic Generation Microscopy

Mol Pharm. 2015 Jul 6;12(7):2378-83. doi: 10.1021/acs.molpharmaceut.5b00065. Epub 2015 Jun 24.

Abstract

Second harmonic generation (SHG) microscopy was used to rapidly identify regions of interest for localized confocal Raman spectroscopy measurements in order to quantify crystallinity within lyophilized Abraxane powder (protein bound paclitaxel for injectable suspension). Water insoluble noncentrosymmetric crystalline particles ranging from ∼1 to 120 μm were identified by SHG, with wide variability in crystal size and frequency observed between several batches of Abraxane. By targeting the Raman analysis to these localized regions identified by SHG, the required measurement time was decreased over 2 orders of magnitude, from 8 h to 2 s. Experimental Raman spectra of SHG active domains in Abraxane were in good agreement with experimental spectra of pure crystalline paclitaxel. These collective results are consistent with up to 30% of the active ingredient being present as poorly soluble crystalline particulates in some batches of Abraxane.

Keywords: Abraxane; Raman spectroscopy; amorphous formulations; lyophilization; microscopy; nanosuspensions; paclitaxel; second harmonic generation.

Publication types

  • Research Support, Non-U.S. Gov't
  • Research Support, U.S. Gov't, Non-P.H.S.

MeSH terms

  • Albumin-Bound Paclitaxel / chemistry
  • Chemistry, Pharmaceutical / methods
  • Microscopy / methods
  • Needles
  • Paclitaxel / chemistry*
  • Particle Size
  • Powders / chemistry
  • Proteins / chemistry*
  • Spectrum Analysis, Raman / methods
  • Suspensions / chemistry

Substances

  • Albumin-Bound Paclitaxel
  • Powders
  • Proteins
  • Suspensions
  • Paclitaxel