9-(3-Bromo-5-chloro-2-hy-droxy-phen-yl)-10-(2-hy-droxy-eth-yl)-3,6-diphenyl-3,4,9,10-tetra-hydro-acridine-1,8(2H,5H)-dione

Mehmet Akkurt; Shaaban K Mohamed; Antar A Abdelhamid; Abdel-Aal M Gaber; Mustafa R Albayati

doi:10.1107/S1600536814010460

9-(3-Bromo-5-chloro-2-hy-droxy-phen-yl)-10-(2-hy-droxy-eth-yl)-3,6-diphenyl-3,4,9,10-tetra-hydro-acridine-1,8(2H,5H)-dione

Acta Crystallogr Sect E Struct Rep Online. 2014 May 17;70(Pt 6):o663-4. doi: 10.1107/S1600536814010460. eCollection 2014 Jun 1.

Authors

Mehmet Akkurt¹, Shaaban K Mohamed², Antar A Abdelhamid³, Abdel-Aal M Gaber⁴, Mustafa R Albayati⁵

Affiliations

¹ Department of Physics, Faculty of Sciences, Erciyes University, 38039 Kayseri, Turkey.
² Chemistry and Environmental Division, Manchester Metropolitan University, Manchester M1 5GD, England ; Chemistry Department, Faculty of Science, Minia University, 61519 El-Minia, Egypt.
³ Chemistry Department, Faculty of Science, Sohag University, 82524 Sohag, Egypt.
⁴ Department of Chemistry, Faculty of Science, Assiut University, 71516 Assiut, Egypt.
⁵ Kirkuk University, College of Science, Department of Chemistry, Kirkuk, Iraq.

Abstract

In the title compound, C33H27BrClNO4, the di-hydro-pyridine ring adopts a flattened boat conformation. The mol-ecular conformation is stabilized by an intra-molecular O-H⋯O hydrogen bond, with an S(8) ring motif. In the crystal, O-H⋯O, C-H⋯O and C-H⋯Cl hydrogen bonds, and C-H⋯π inter-actions link the mol-ecules, forming a three-dimensional network. In the acridinedione ring system, the two ring C atoms at the 2- and 3-positions, and the C atom at the 6-position and the atoms of the phenyl ring attached to the C atom at the 6-position are disordered over two sets of sites with occupancy ratios of 0.783 (5):0.217 (5) and 0.526 (18):0.474 (18), respectively.