N,N'-(Propane-1,3-di-yl)dibenzo-thio-amide

Masayuki Nagasawa; Yuji Sasanuma; Hyuma Masu

doi:10.1107/S160053681400974X

N,N'-(Propane-1,3-di-yl)dibenzo-thio-amide

Acta Crystallogr Sect E Struct Rep Online. 2014 May 3;70(Pt 6):o639. doi: 10.1107/S160053681400974X. eCollection 2014 Jun 1.

Authors

Masayuki Nagasawa¹, Yuji Sasanuma¹, Hyuma Masu²

Affiliations

¹ Department of Applied Chemistry and Biotechnology, Chiba University, 1-33 Yayoi-cho, Inage-ku, Chiba 263-8522, Japan.
² Center for Analytical Instrumentation, Chiba University, 1-33 Yayoi-cho, Inage-ku, Chiba 263-8522, Japan.

Abstract

The title compound, C17H18N2S2, exhibits a trans-trans-trans-gauche(+) (tttg (+)) conformation with regard to the NH-CH2-CH2-CH2-NH bond sequence. In the crystal, mol-ecules are connected by N-H⋯S=C and C-H⋯S=C hydrogen bonds, forming a herringbone arrangement along the c-axis direction. The two thioamide groups make dihedral angles of 43.0 (2) and 33.1 (2)° with the adjacent phenyl rings.