Mapping of an ultrasonic bath for ultrasound assisted extraction of mangiferin from Mangifera indica leaves

Ultrason Sonochem. 2014 Mar;21(2):606-11. doi: 10.1016/j.ultsonch.2013.08.021. Epub 2013 Sep 7.

Abstract

The present work deals with the mapping of an ultrasonic bath for the maximum extraction of mangiferin from Mangifera indica leaves. I3(-) liberation experiments (chemical transformations) and extraction (physical transformations) were carried out at different locations in an ultrasonic bath and compared. The experimental findings indicated a similar trend in variation in an ultrasonic bath by both these methods. Various parameters such as position and depth of vessel in an ultrasonic bath, diameter and shape of a vessel, frequency and input power which affect the extraction yield have been studied in detail. Maximum yield of mangiferin obtained was approximately 31 mg/g at optimized parameters: distance of 2.54 cm above the bottom of the bath, 7 cm diameter of vessel, flat bottom vessel, 6.35 cm liquid height, 122 W input power and 25 kHz frequency. The present work indicates that the position and depth of vessel in an ultrasonic bath, diameter and shape of a vessel, frequency and input power have significant effect on the extraction yield. This work can be used as a base for all ultrasonic baths to obtain maximum efficiency for ultrasound assisted extraction.

Keywords: Extraction; Mangiferin; Mapping; Natural products; Ultrasonic bath.

MeSH terms

  • Chemical Fractionation / methods*
  • Mangifera / chemistry*
  • Plant Leaves / chemistry*
  • Transducers
  • Ultrasonics / instrumentation
  • Ultrasonics / methods*
  • Xanthones / isolation & purification*

Substances

  • Xanthones
  • mangiferin