Grazing-incidence X-ray diffraction of single GaAs nanowires at locations defined by focused ion beams

J Appl Crystallogr. 2013 Aug 1;46(Pt 4):887-892. doi: 10.1107/S0021889813004226. Epub 2013 Jun 7.

Abstract

Grazing-incidence X-ray diffraction measurements on single GaAs nanowires (NWs) grown on a (111)-oriented GaAs substrate by molecular beam epitaxy are reported. The positions of the NWs are intentionally determined by a direct implantation of Au with focused ion beams. This controlled arrangement in combination with a nanofocused X-ray beam allows the in-plane lattice parameter of single NWs to be probed, which is not possible for randomly grown NWs. Reciprocal space maps were collected at different heights along the NW to investigate the crystal structure. Simultaneously, substrate areas with different distances from the Au-implantation spots below the NWs were probed. Around the NWs, the data revealed a 0.4% decrease in the lattice spacing in the substrate compared with the expected unstrained value. This suggests the presence of a compressed region due to Au implantation.

Keywords: GaAs; grazing-incidence X-ray diffraction; growth; semiconductor nanowires.