1,3,5-Tris(4-bromo-phen-yl)-1,3,5-triazin-ane di-chloro-methane monosolvate

Mahmoud Chebbah; Ahcene Bouchemma; Sofiane Bouacida; Leila Lefrada; Mustapha Bouhenguel

doi:10.1107/S1600536813013743

1,3,5-Tris(4-bromo-phen-yl)-1,3,5-triazin-ane di-chloro-methane monosolvate

Acta Crystallogr Sect E Struct Rep Online. 2013 May 25;69(Pt 6):o976. doi: 10.1107/S1600536813013743. Print 2013 Jun 1.

Authors

Mahmoud Chebbah¹, Ahcene Bouchemma, Sofiane Bouacida, Leila Lefrada, Mustapha Bouhenguel

Affiliation

¹ Laboratoire de Chimie Appliquée et Technologie des Matériaux LCATM, Université Oum El Bouaghi, Algeria ; Département Sciences de la Matière, Faculté des Sciences Exactes et Sciences de la Nature et de la Vie, Université Oum El Bouaghi, Algeria.

Abstract

In the main mol-ecule of the title compound, C21H18Br3N3·CH2Cl2, the triazinane ring adopts a chair conformation with three 4-brom-ophenyl substituents, two in diaxial positions and the third in an equatorial arrangement (eaa). The torsion angles around the N-C bonds in the triazinane ring are in the range 55.6 (5)-60.1 (5)°. The structure can be described as being built up of alternating layers along the b axis with the CH2Cl2 solvent mol-ecules sandwiched between these layers. No classical hydrogen-bonding inter-actions are observed in the crystal structure.