Effect of different irrigation protocols on resin sealer bond strength to dentin

J Endod. 2013 May;39(5):689-92. doi: 10.1016/j.joen.2012.12.009. Epub 2013 Feb 7.

Abstract

Introduction: The aim of this study was to evaluate the influence of different irrigation protocols on resin-based sealer bond strength to dentin and the associated failure pattern.

Methods: One hundred eighty single-rooted premolars were used. Roots were divided into 18 groups according to the irrigation protocol used and instrumented using 5.25% NaOCl or 2% chlorhexidine (CHX) gel as chemical auxiliary substances and 17% EDTA or 37% phosphoric acid for smear layer removal. Finally, CHX solution was used as the final irrigant in some groups. Root canals were filled with either gutta-percha and AH Plus (Dentsply, Petropolis, RJ, Brazil) (GP/AH) or Resilon/Real Seal SE (SybronEndo, Orange, CA). Bond strength was measured by the push-out test. Additionally, failure patterns were classified as adhesive, cohesive, and mixed. Data were statistically analyzed by Kruskal-Wallis and Mann-Whitney U tests.

Results: In the GP/AH groups, high bond strength values were obtained when NaOCl was associated with phosphoric acid with (6.9 ± 3.9) and without (7.4 ± 3.8) a final flush with CHX. However, when CHX gel was used, the association with EDTA with (7.5 ± 3.2) and without (6.0 ± 2.3) a final flush with CHX solution showed better results. The GP/AH groups mainly showed a cohesive failure pattern. Evaluation of Resilon/Real Seal SE showed that higher bond strength values were reached when CHX was associated with phosphoric acid with (5.2 ± 3.0) and without (4.2 ± 2.0) a final flush with CHX solution. The failure patterns were mainly adhesive.

Conclusions: Irrigation protocols influenced the bond strength of resin sealers to dentin.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Adhesiveness
  • Bicuspid / ultrastructure
  • Chlorhexidine / chemistry
  • Composite Resins / chemistry
  • Dental Bonding*
  • Dental Pulp Cavity / ultrastructure*
  • Dental Stress Analysis / instrumentation
  • Dentin / ultrastructure*
  • Edetic Acid / chemistry
  • Epoxy Resins / chemistry
  • Gutta-Percha / chemistry
  • Humans
  • Materials Testing
  • Phosphoric Acids / chemistry
  • Root Canal Filling Materials / chemistry*
  • Root Canal Irrigants / chemistry*
  • Root Canal Preparation / instrumentation
  • Smear Layer
  • Sodium Hypochlorite / chemistry
  • Stress, Mechanical
  • Therapeutic Irrigation / methods*
  • Tooth Apex / ultrastructure

Substances

  • Composite Resins
  • Epoxy Resins
  • Phosphoric Acids
  • Real Seal composite resin
  • Root Canal Filling Materials
  • Root Canal Irrigants
  • epoxy resin-based root canal sealer
  • resilon sealer
  • Gutta-Percha
  • Edetic Acid
  • Sodium Hypochlorite
  • phosphoric acid
  • Chlorhexidine