A microfocus X-ray fluorescence beamline at Indus-2 synchrotron radiation facility

J Synchrotron Radiat. 2013 Mar;20(Pt 2):386-9. doi: 10.1107/S0909049513001337. Epub 2013 Feb 2.

Abstract

A microfocus X-ray fluorescence spectroscopy beamline (BL-16) at the Indian synchrotron radiation facility Indus-2 has been constructed with an experimental emphasis on environmental, archaeological, biomedical and material science applications involving heavy metal speciation and their localization. The beamline offers a combination of different analytical probes, e.g. X-ray fluorescence mapping, X-ray microspectroscopy and total-external-reflection fluorescence characterization. The beamline is installed on a bending-magnet source with a working X-ray energy range of 4-20 keV, enabling it to excite K-edges of all elements from S to Nb and L-edges from Ag to U. The optics of the beamline comprises of a double-crystal monochromator with Si(111) symmetric and asymmetric crystals and a pair of Kirkpatrick-Baez focusing mirrors. This paper describes the performance of the beamline and its capabilities with examples of measured results.

Keywords: X-ray fluorescence; X-ray microscopy; X-ray scattering; microprobe.

MeSH terms

  • Crystallography, X-Ray / methods
  • Equipment Design
  • India
  • Plant Leaves / chemistry
  • Solanum lycopersicum / chemistry
  • Spectrometry, X-Ray Emission / methods
  • Synchrotrons / instrumentation*