Achieving high resolution dipolar NMR information without fast sample spinning: combining magic angle turning with dipolar based NMR methods

A Ananthanarayanan; L van Wüllen

doi:10.1016/j.ssnmr.2012.11.005

Achieving high resolution dipolar NMR information without fast sample spinning: combining magic angle turning with dipolar based NMR methods

Solid State Nucl Magn Reson. 2013 Feb:49-50:42-6. doi: 10.1016/j.ssnmr.2012.11.005. Epub 2012 Dec 3.

Authors

A Ananthanarayanan¹, L van Wüllen

Affiliation

¹ Institute of Physics, Augsburg University, Universitätsstr. 1, D-86159 Augsburg, Germany.

PMID: 23290723
DOI: 10.1016/j.ssnmr.2012.11.005

Abstract

In this article we present a new approach to high resolution NMR combining the concepts of magic angle hopping (MAH)/magic angle turning (MAT) and dipolar based NMR methods such as SEDOR, REDOR or cross polarization (CP). Employing aluminophosphates as model systems we demonstrate that No MAS needed (NOMAS) is capable of supplying high resolution dipolar information without the need of fast MAS.

Publication types

Research Support, Non-U.S. Gov't