In situ reaction furnace for real-time XRD studies

J Synchrotron Radiat. 2013 Jan;20(Pt 1):194-6. doi: 10.1107/S0909049512039246. Epub 2012 Nov 10.

Abstract

The new furnace at the Materials Characterization by X-ray Diffraction beamline at Elettra has been designed for powder diffraction measurements at high temperature (up to 1373 K at the present state). Around the measurement region the geometry of the radiative heating element assures a negligible temperature gradient along the capillary and can accommodate either powder samples in capillary or small flat samples. A double capillary holder allows flow-through of gas in the inner sample capillary while the outer one serves as the reaction chamber. The furnace is coupled to a translating curved imaging-plate detector, allowing the collection of diffraction patterns up to 2θ ≃ 130°.