An effective method for the fabrication of few-layer-thick inorganic nanosheets

Angew Chem Int Ed Engl. 2012 Sep 3;51(36):9052-6. doi: 10.1002/anie.201204208. Epub 2012 Aug 9.

Abstract

Intercalation and exfoliation of lithium: Few-layer-thick inorganic nanosheets (BN, NbSe(2), WSe(2), Sb(2)Se(3), and Bi(2)Te(3)) have been prepared from their layered bulk precursors by using a controllable electrochemical lithium intercalation process. The lithium intercalation conditions, such as cut-off voltage and discharge current, have been systematically studied and optimized to produce high-quality BN and NbSe(2) nanosheets.