Synthesis and NMR spectral studies of the 7-C₆₀-adduct of n,n-(tetrachlorophthaloyl) dehydroabietylamine

Molecules. 2012 Apr 5;17(4):4209-18. doi: 10.3390/molecules17044209.

Abstract

The 7-C₆₀-adduct of N,N-(tetrachlorophthaloyl)dehydroabietylamine was synthesized for the first time and characterized by IR, UV-vis, mass and NMR spectral studies. The ¹H-NMR and ¹³C-NMR resonance signals of the new compound are unambiguously assigned by using homo- and heteronuclear 2D NMR spectroscopic techniques such as COSY, ROESY, HSQC and HMBC. The C₁ symmetric structure with 6,6-junction of compound was determined.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Carbon / chemistry
  • Carbon Isotopes
  • Diterpenes / analysis
  • Diterpenes / chemical synthesis
  • Diterpenes / chemistry*
  • Nuclear Magnetic Resonance, Biomolecular
  • Phthalic Acids / analysis
  • Phthalic Acids / chemical synthesis
  • Phthalic Acids / chemistry*

Substances

  • 7-C60-adduct of N,N-(tetrachlorophthaloyl)dehydroabietylamine
  • Carbon Isotopes
  • Diterpenes
  • Phthalic Acids
  • Carbon