2-(Naphthalen-1-yl-amino)-cyclo-hexa-nol

Acta Crystallogr Sect E Struct Rep Online. 2011 Jul 1;67(Pt 7):o1628. doi: 10.1107/S1600536811021714. Epub 2011 Jun 11.

Abstract

The title compound, C(16)H(19)NO, was synthesized under solvent-free conditions by reaction of 7-oxa-bicyclo-[4.1.0]heptane and naphthalen-1-amine in the presence of Ca(CF(3)COO)(2) as catalyst. The cyclo-hexane ring adopts a chair conformation. In the crystal, mol-ecules are linked by inter-molecular N-H⋯O hydrogen bonds and C-H⋯π inter-actions into chains parallel to the c axis.