Synthesis, growth, crystal structure and characterization of a new organic material: glycine glutaric acid

Spectrochim Acta A Mol Biomol Spectrosc. 2011 Jan;78(1):543-8. doi: 10.1016/j.saa.2010.11.026. Epub 2010 Nov 26.

Abstract

Glycine glutaric acid, a new organic compound has been synthesized and good quality single crystals were grown by slow evaporation technique. The structure of the grown crystal was elucidated by using single crystal XRD. The presence of the functional groups was confirmed by using FT-IR spectroscopy. The optical transparency was studied by using UV-vis spectrophotometer and it was found that the crystal is having high optical transparency. The thermal stability of the crystal was studied by using thermo-gravimetric and differential thermal analyses and found that it is stable up to 150°C. The room temperature dielectric studies were also carried out over the wide frequency range: 10 mHz to 10 MHz.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Absorption
  • Crystallization
  • Crystallography, X-Ray
  • Dielectric Spectroscopy
  • Glutarates / chemical synthesis*
  • Glutarates / chemistry*
  • Glycine / chemical synthesis*
  • Glycine / chemistry*
  • Hydrogen Bonding
  • Molecular Conformation
  • Solubility
  • Spectrophotometry, Ultraviolet
  • Spectroscopy, Fourier Transform Infrared
  • Temperature
  • Thermogravimetry

Substances

  • Glutarates
  • glutaric acid
  • Glycine