[Studies on the chemical constituents of ethyl acetate extraction from Reineckea carnea]

Zhong Yao Cai. 2009 Sep;32(9):1402-4.
[Article in Chinese]

Abstract

Objective: To study the chemical constituents of Reineckea carnea.

Methods: The compounds were isolated by extraction, silica gel and reversed phase silica gel column chromatography. The structures were identified by various spectroscopic methods including 1D and 2D-NMR spectrum, MS, IR, etc.

Results: Six compounds were isolated and identified as beta-sitosterol (1), isorhodeasapogenin (2), isorhodeasapogenin (3), (25S)-1beta,3beta,4beta-trihydroxyspirotan-5beta-yl-O-beta-D-glucopyranoside (4), kitigenin-5-O-beta-D-glucopyranoside (5) and nicotianoside B (6).

Conclusion: Compounds 4, 6 are obtained from this plant for the first time.

Publication types

  • English Abstract

MeSH terms

  • Acetates
  • Drugs, Chinese Herbal / chemistry*
  • Glucosides / chemistry
  • Glucosides / isolation & purification*
  • Liliaceae / chemistry*
  • Magnetic Resonance Spectroscopy
  • Plants, Medicinal / chemistry*
  • Rhizome / chemistry
  • Saponins / chemistry
  • Saponins / isolation & purification*
  • Sitosterols / chemistry
  • Sitosterols / isolation & purification
  • Spectrophotometry, Infrared
  • Steroids / chemistry
  • Steroids / isolation & purification*

Substances

  • Acetates
  • Drugs, Chinese Herbal
  • Glucosides
  • Saponins
  • Sitosterols
  • Steroids
  • hemeroside B
  • gamma-sitosterol
  • ethyl acetate