Large-volume sample stacking for the analysis of seven beta-lactam antibiotics in milk samples of different origins by CZE

Electrophoresis. 2007 Nov;28(22):4082-90. doi: 10.1002/elps.200700305.

Abstract

A method for the simultaneous determination of eight beta-lactam antibiotics (nafcillin, cloxacillin, oxacillin, dicloxacillin, ampicillin, amoxicillin, and penicillin G) in fortified milk samples of different origins has been proposed by using CZE with diode-array detection (CZE-DAD). Optimum separation was obtained on a 64.5 cm x 75 microm bubble cell capillary using 175 mM Tris buffer with 20% ethanol at pH 8.0. Methylparaben has been used as an internal standard (IS). Taking into account the lack of sensitivity of the UV-Vis detection, a solvent extraction/SPE method was applied for off-line preconcentration and sample cleanup, and also an on-line preconcentration methodology, such as large-volume sample stacking (LVSS) with polarity switching, was developed, providing LODs ranging from 2 to 10 microg/L. The method permits the quantification of these residues below the levels established in milk by the EU Regulation. Satisfactory recoveries ranging from 86 to 93% were also obtained in milk samples of different origins.

Publication types

  • Evaluation Study
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Animals
  • Anti-Bacterial Agents / analysis*
  • Electrophoresis, Capillary / methods*
  • Food Analysis / methods
  • Food Contamination / analysis*
  • Maximum Allowable Concentration
  • Milk / chemistry*
  • Milk / standards
  • beta-Lactams / analysis*

Substances

  • Anti-Bacterial Agents
  • beta-Lactams