In-situ hydration studies using multi-angle energy-dispersive diffraction

J Synchrotron Radiat. 1998 Mar 1;5(Pt 2):112-7. doi: 10.1107/S0909049597018712.

Abstract

A new diffractometer has been built with which energy-dispersive diffraction patterns can be collected simultaneously at different angles. The first use of this system for dynamic (time-resolved) studies--the hydration of cements under various conditions--is reported. It is found that the optimization available with a three-element detector system enables collection of high-quality patterns over a much wider and more effective range of reciprocal space, and this yields improved and new information on the hydration processes.