Editing of H2BC NMR spectra

Magn Reson Chem. 2005 Dec;43(12):971-4. doi: 10.1002/mrc.1698.

Abstract

New versions of the H2BC pulse sequence (Nyberg NT, Duus JØ, Sørensen OW. J. Am. Chem. Soc. 2005; 127: 6154) that edit into two subspectra according to the number of protons attached to 13C nuclei being odd or even are introduced. These sequences can be useful for resolving spectral overlap, which is demonstrated on the molecule prednisolone [(11 beta)-11,17,21-trihydroxypregna-1,4-diene-3,20-dione].

MeSH terms

  • Magnetic Resonance Spectroscopy / methods*
  • Prednisolone / chemistry

Substances

  • Prednisolone