In situ ESEM observation of melting silver and Inconel on an Al(2)O(3) powder bed

J Electron Microsc (Tokyo). 2004;53(4):393-6. doi: 10.1093/jmicro/dfh070.

Abstract

A hot stage in an environmental scanning electron microscope (ESEM) was used for in situ infiltration experiments. Pressureless infiltration of a porous Ti-activated Al(2)O(3) preform has been investigated at temperatures up to 1530 degrees C under two atmospheres (He and H(2)O((g))). A brief description of the operating and the experimental set-up is given. Silver and Inconel (Ni superalloy) infiltration experiments demonstrate the in situ potential of the ESEM at temperatures up to 1500 degrees C.

MeSH terms

  • Alloys / chemistry*
  • Aluminum / chemistry*
  • Helium / chemistry*
  • Microscopy, Electron, Scanning
  • Silver / chemistry*
  • Temperature

Substances

  • Alloys
  • Helium
  • Silver
  • Aluminum