Stereoselective polymerization of rac-lactide using a monoethylaluminum Schiff base complex

Biomacromolecules. 2004 May-Jun;5(3):965-70. doi: 10.1021/bm034467o.

Abstract

A monoethylaluminum Schiff base complex (2) with formula LAlEt (L = N,N'-(2,2-dimethylpropylene)bis(3,5-di-tert-butylsalicylideneimine) was synthesized and employed for the stereoselective ring-opening polymerization of rac-lactide (rac-LA). The complex 2 was characterized by nuclear magnetic resonance, crystal structure, and elemental analysis. It contains a five-coordinate aluminum atom with distorted trigonal bipyramidal geometry in the solid state. In the presence of 2-propanol, 2 showed high stereoselectivity for the polymerization of rac-LA. The polymerization yielded crystalline poly(rac-LA) with a high melting temperature (193-201 degrees C). NMR, differential scanning calorimetry, and wide-angle X-ray diffraction indicated that the poly(rac-LA) was highly isotactic, and a stereocomplex was formed between poly-l- and poly-d-lactide block sequences. By the analysis of electrospray-ionization mass spectrometry and (1)H NMR, the polymer was demonstrated to be endcapped in both terminals with an isopropyl ester and a hydroxy group, respectively. The polymerization was of first order in rac-LA concentration. The relationship between the rac-LA conversion and molecular weights of the polymer was linear so that the polymerization could be well controlled.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Aluminum Compounds / chemistry*
  • Calorimetry, Differential Scanning
  • Magnetic Resonance Spectroscopy
  • Polyesters / chemistry*
  • Schiff Bases / chemistry*
  • Stereoisomerism
  • X-Ray Diffraction

Substances

  • Aluminum Compounds
  • Polyesters
  • Schiff Bases
  • poly(lactide)