Dispiro[adamantane-2,2'-1',3',6',9',11',14'-hexathiacyclohexadecane-10',2"-adamantane]

Aleksandar Visnjevac; Biserka Kojić-Prodić; Marijana Vinković; Kata Mlinarić-Majerski

doi:10.1107/s0108270103008369

Dispiro[adamantane-2,2'-1',3',6',9',11',14'-hexathiacyclohexadecane-10',2"-adamantane]

Acta Crystallogr C. 2003 Jun;59(Pt 6):o314-6. doi: 10.1107/s0108270103008369. Epub 2003 May 20.

Authors

Aleksandar Visnjevac¹, Biserka Kojić-Prodić, Marijana Vinković, Kata Mlinarić-Majerski

Affiliation

¹ Rudjer Bosković Institute, PO Box 180, HR-10002 Zagreb, Croatia. aleksandar.visnjevac@irb.hr

PMID: 12794349
DOI: 10.1107/s0108270103008369

Abstract

The conformational features of the title compound, C(28)H(44)S(6), are compared with previously reported analogous macrocycles. The type of substituent affects considerably the conformation of the macrocycle. A (1)H NMR titration of the title compound with AgBF(4) indicated the formation of the 1:1 complex, which was not crystallized.